Nano-Gold Corking and Enzymatic Uncorking of Carbon Nanotube Cups.

Because of their unique stacked, cup-shaped, hollow compartments, nitrogen-doped carbon nanotube cups (NCNCs) have promising potential as nanoscale containers. Individual NCNCs are isolated from their stacked structure through acid oxidation and subsequent probe-tip sonication. The NCNCs are then ef...

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Publicado en:Journal of the American Chemical Society Vol. 137; no. 2; pp. 675 - 685
Autores principales: Yong Zhao, Burkert, Seth C., Yifan Tang, Sorescu, Dan C., Kapralov, Alexandr A., Shurin, Galina V., Shurin, Michael R., Kagan, Valerian E., Star, Alexander
Formato: Artículo
Publicado: American Chemical Society 1/21/2015
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Acceso en línea:Ver este registro en EBSCOhost
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      dt: 1/21/2015
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        10.1021/ja511843w
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        atl: Nano-Gold Corking and Enzymatic Uncorking of Carbon Nanotube Cups.
      aug:
        au:
          Yong Zhao
          Burkert, Seth C.
          Yifan Tang
          Sorescu, Dan C.
          Kapralov, Alexandr A.
          Shurin, Galina V.
          Shurin, Michael R.
          Kagan, Valerian E.
          Star, Alexander
        affil:
          Department of Chemistry, University of Pittsburgh, Pittsburgh, Pennsylvania 15260, United States
          National Energy Technology Laboratory, U.S. Department of Energy, Pittsburgh, Pennsylvania 15263, United States
          Department of Environmental and Occupational Health, University of Pittsburgh, Pittsburgh, Pennsylvania 15261, United States
          Department of Pathology, University of Pittsburgh Medical Center, Pittsburgh, Pennsylvania 15261, United States
          Department of Immunology, University of Pittsburgh Medical Center, Pittsburgh, Pennsylvania 15261, United States
      su:
        Carbon nanotubes
        Nucleation
        Gold nanoparticles
        Raman microscopy
        Nanocapsules
        Density functional theory
      sug:
        subj:
          Carbon nanotubes
          Nucleation
          Gold nanoparticles
          Raman microscopy
          Nanocapsules
          Density functional theory
      ab: Because of their unique stacked, cup-shaped, hollow compartments, nitrogen-doped carbon nanotube cups (NCNCs) have promising potential as nanoscale containers. Individual NCNCs are isolated from their stacked structure through acid oxidation and subsequent probe-tip sonication. The NCNCs are then effectively corked with gold nanoparticles (GNPs) by sodium citrate reduction with chloroauric acid, forming graphitic nanocapsules with significant surface-enhanced Raman signature. Mechanistically, the growth of the GNP corks starts from the nucleation and welding of gold seeds on the open rims of NCNCs enriched with nitrogen functionalities, as confirmed by density functional theory calculations. A potent oxidizing enzyme of neutrophils, myeloperoxidase (MPO), can effectively open the corked NCNCs through GNP detachment, with subsequent complete enzymatic degradation of the graphitic shells. This controlled opening and degradation was further carried out in vitro with human neutrophils. Furthermore, the GNP-corked NCNCs were demonstrated to function as novel drug delivery carriers, capable of effective (i) delivery of paclitaxel to tumor-associated myeloid-derived suppressor cells (MDSC), (ii) MPO-regulated release, and (iii) blockade of MDSC immunosuppressive potential.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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          year: 2015
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