Efficient Catalyst One-Pot Synthesis of 7-(Aryl)-10,10-dimethyl-10,11-dihydrochromeno[4,3-b]chromene-6,8(7H,9H)-dione Derivatives Complemented by Antibacterial Activity.

The problem of bacteria resistance to many known agents has inspired scientists and researchers to discover novel efficient antibacterial drugs. Three rapid, clean, and highly efficient methods were developed for one-pot synthesis of 7-(aryl)-10,10-dimethyl-10,11-dihydrochromeno[4,3-b]chromene-6,8(7...

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Publicado en:BioMed Research International Vol. 2016; pp. 1 - 8
Autores principales: Al-Majedy, Yasameen K., Al-Amiery, Ahmed A., Kadhum, Abdul Amir H., Mohamad, Abu Bakar
Formato: equations & formulas pictorial research tables/charts Journal Article
Publicado: Wiley-Blackwell 7/31/2016
Acceso en línea:Ver este registro en EBSCOhost
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      dt: 7/31/2016
      vid: 2016
      pid: 480
      pub: Wiley-Blackwell
      place: Malden, Massachusetts
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        117105038
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        117105038
        10.1155/2016/5891703
        117105038
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        atl: Efficient Catalyst One-Pot Synthesis of 7-(Aryl)-10,10-dimethyl-10,11-dihydrochromeno[4,3-b]chromene-6,8(7H,9H)-dione Derivatives Complemented by Antibacterial Activity.
      aug:
        au:
          Al-Majedy, Yasameen K.
          Al-Amiery, Ahmed A.
          Kadhum, Abdul Amir H.
          Mohamad, Abu Bakar
        affil: Department of Chemical and Process Engineering, Universiti Kebangsaan Malaysia (UKM), 43000 Bangi, Selangor, Malaysia
      sug:
        subj:
          Antibiotics Analysis
          Benzopyrans Analysis
          Bacterial Infections Drug Therapy
          Antibiotics Administration and Dosage
          Benzopyrans Administration and Dosage
          Chemistry
          Molecular Structure
          Drug Resistance, Microbial
          Aldehydes
          Bromides
          Phosphates
          Chlorides
          Technology, Pharmaceutical
          Magnetic Resonance Spectroscopy Methods
          Antioxidants Analysis
          Staphylococcus Aureus Drug Effects
          Streptococcus Drug Effects
          Pseudomonas Drug Effects
          Proteus Drug Effects
          Free Radical Scavengers
          Biological Assay
          Chromatography, Thin Layer
          Spectrophotometry, Infrared
          Dimethyl Sulfoxide
          Descriptive Statistics
          One-Way Analysis of Variance
          Data Analysis Software
          P-Value
          Funding Source
      ab: The problem of bacteria resistance to many known agents has inspired scientists and researchers to discover novel efficient antibacterial drugs. Three rapid, clean, and highly efficient methods were developed for one-pot synthesis of 7-(aryl)-10,10-dimethyl-10,11-dihydrochromeno[4,3-b]chromene-6,8(7H,9H)-dione derivatives. Three components are condensed in the synthesis, 4-hydroxycoumarin, 5,5-dimethyl-1,3-cyclohexanedione, and aromatic aldehydes, using tetrabutylammonium bromide (TBAB), diammonium hydrogen phosphate (DAHP), or ferric chloride (FeCl3), respectively. Each method has different reaction mechanisms according to the catalyst. The present methods have advantages, including one-pot synthesis, excellent yields, short reaction times, and easy isolation of product. All catalysts utilized in our study could be reused several times without losing their catalytic efficiency. All synthesized compounds were fully characterized and evaluated for their antibacterial activity.
      pubtype: Academic Journal
      doctype:
        equations & formulas
        pictorial
        research
        tables/charts
        Journal Article
      ougenre: Article
    language: English
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