Deciphering the Spatial Arrangement of Metals and Correlation to Reactivity in Multivariate Metal-Organic Frameworks.

Thirty-six porphyrin-based metal–organic frameworks (MOFs) with composition of (MO)(TCPP-M) and MO trigonal SBUs of various metals, MgO, MnO, CoO, NiO, and FeO including mixed-metal SBUs, MnFeO, NiFeO, CoNiO, MnCoO, MnMgO, and MnNiO were synthesized and characterized. These multivariate MOFs (MTV-MO...

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Publicado en:Journal of the American Chemical Society Vol. 138; no. 42; pp. 13822 - 13826
Autores principales: Qi Liu, Hengjiang Cong, Hexiang Deng
Formato: Artículo
Publicado: American Chemical Society 10/26/2016
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Acceso en línea:Ver este registro en EBSCOhost
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      pub: American Chemical Society
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        10.1021/jacs.6b08724
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        atl: Deciphering the Spatial Arrangement of Metals and Correlation to Reactivity in Multivariate Metal-Organic Frameworks.
      aug:
        au:
          Qi Liu
          Hengjiang Cong
          Hexiang Deng
        affil:
          Key Laboratory of Biomedical Polymers-Ministry of Education, College of Chemistry and Molecular Sciences, Wuhan University, Wuhan 430072, China.
          The Institute for Advanced Studies, Wuhan University, Wuhan 430072, China.
      su:
        Metals
        Structural frames
        Metallic oxides
        Porphyrins
        Space groups
      sug:
        subj:
          Metals
          Structural frames
          Metallic oxides
          Porphyrins
          Space groups
      ab: Thirty-six porphyrin-based metal–organic frameworks (MOFs) with composition of (MO)(TCPP-M) and MO trigonal SBUs of various metals, MgO, MnO, CoO, NiO, and FeO including mixed-metal SBUs, MnFeO, NiFeO, CoNiO, MnCoO, MnMgO, and MnNiO were synthesized and characterized. These multivariate MOFs (MTV-MOFs) were examined by X-ray photoelectron spectroscopy, UV–vis diffuse reflectance spectra, and for the first time, their metal spatial arrangement deciphered and were found to exist in the form of either domains or well-mixed. We find that MTV-MOFs with well-mixed metals in their SBUs, rather than the SBUs having one kind of metal but different from one SBU to another, perform better than the sum of their parts in the test reaction involving the photo-oxidation of 1,5-dihydroxynaphthalene.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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