Carbon dioxide sequestration using NaHSO4 and NaOH: A dissolution and carbonation optimisation study.

The use of NaHSO 4 to leach out Mg fromlizardite-rich serpentinite (in form of MgSO 4 ) and the carbonation of CO 2 (captured in form of Na 2 CO 3 using NaOH) to form MgCO 3 and Na 2 SO 4 was investigated. Unlike ammonium sulphate, sodium sulphate can be separated via precipitation during the recycl...

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Publicado en:Journal of Environmental Management Vol. 189; pp. 84 - 98
Autores principales: Sanna, Aimaro, Steel, Luc, Maroto-Valer, M. Mercedes
Formato: Artículo
Publicado: Academic Press Inc. Mar2017
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Acceso en línea:Ver este registro en EBSCOhost
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        03014797
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      jtl: Journal of Environmental Management
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      dt: Mar2017
      vid: 189
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      pub: Academic Press Inc.
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        120589352
        10.1016/j.jenvman.2016.12.029
      ppf: 84
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        atl: Carbon dioxide sequestration using NaHSO4 and NaOH: A dissolution and carbonation optimisation study.
      aug:
        au:
          Sanna, Aimaro
          Steel, Luc
          Maroto-Valer, M. Mercedes
        affil: Centre for Innovation in Carbon Capture and Storage (CICCS), Institute of Mechanical, Process and Energy Engineering (IMPEE), School of Engineering & Physical Sciences, Heriot-Watt University, Edinburgh, EH14 4AS, UK
      su:
        Carbon sequestration
        Sodium hydroxide
        Sodium sulfate
        Dissolution (Chemistry)
        Carbonation (Chemistry)
        Precipitation (Chemistry)
      sug:
        subj:
          Chemical (except agricultural) and allied product merchant wholesalers
          Alkali and chlorine manufacturing
          Other Chemical and Allied Products Merchant Wholesalers
          Other Basic Inorganic Chemical Manufacturing
          All other non-metallic mineral mining and quarrying
          All other basic inorganic chemical manufacturing
          Potash, Soda, and Borate Mineral Mining
          Carbon sequestration
          Sodium hydroxide
          Sodium sulfate
          Dissolution (Chemistry)
          Carbonation (Chemistry)
          Precipitation (Chemistry)
      keyword:
        CCS
        Clean energy
        CO 2 fixation
        Mineral carbonation
        Sodium salts
        CCS
        Clean energy
        CO 2 fixation
        Mineral carbonation
        Sodium salts
      ab: The use of NaHSO 4 to leach out Mg fromlizardite-rich serpentinite (in form of MgSO 4 ) and the carbonation of CO 2 (captured in form of Na 2 CO 3 using NaOH) to form MgCO 3 and Na 2 SO 4 was investigated. Unlike ammonium sulphate, sodium sulphate can be separated via precipitation during the recycling step avoiding energy intensive evaporation process required in NH 4 -based processes. To determine the effectiveness of the NaHSO 4 /NaOH process when applied to lizardite, the optimisation of the dissolution and carbonation steps were performed using a UK lizardite-rich serpentine. Temperature, solid/liquid ratio, particle size, concentration and molar ratio were evaluated. An optimal dissolution efficiency of 69.6% was achieved over 3 h at 100 °C using 1.4 M sodium bisulphate and 50 g/l serpentine with particle size 75–150 μm. An optimal carbonation efficiency of 95.4% was achieved over 30 min at 90 °C and 1:1 magnesium:sodium carbonate molar ratio using non-synthesised solution. The CO 2 sequestration capacity was 223.6 g carbon dioxide/kg serpentine (66.4% in terms of Mg bonded to hydromagnesite), which is comparable with those obtained using ammonium based processes. Therefore, lizardite-rich serpentinites represent a valuable resource for the NaHSO 4 /NaOH based pH swing mineralisation process.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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