Dynamic Stabilization of Metal Oxide-Water Interfaces.

The interaction of water with metal oxide surfaces plays a crucial role in the catalytic and geochemical behavior of metal oxides. In a vast majority of studies, the interfacial structure is assumed to arise from a relatively static lowest energy configuration of atoms, even at room temperature. Usi...

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Publicado en:Journal of the American Chemical Society Vol. 139; no. 7; pp. 2581 - 2585
Autores principales: Mcbriarty, Martin E., Von Rudorff, Guido Falk, Stubbs, Joanne E., Eng, Peter J., Blumberger, Jochen, Rosso, Kevin M.
Formato: Artículo
Publicado: American Chemical Society 2/22/2017
Materias:
Acceso en línea:Ver este registro en EBSCOhost
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        10.1021/jacs.6b13096
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        atl: Dynamic Stabilization of Metal Oxide-Water Interfaces.
      aug:
        au:
          Mcbriarty, Martin E.
          Von Rudorff, Guido Falk
          Stubbs, Joanne E.
          Eng, Peter J.
          Blumberger, Jochen
          Rosso, Kevin M.
        affil:
          Physical Sciences Division, Pacific Northwest National Laboratory, Richland, Washington 99352, United States
          Department of Physics and Astronomy, University College London, London WC1E 6BT, U.K.
          Center for Advanced Radiation Sources, University of Chicago, Chicago, Illinois 60439, United States
      su:
        Metallic oxides
        Hematite
        X-ray scattering
        Density functional theory
        Simulation methods & models
      sug:
        subj:
          Metallic oxides
          Hematite
          X-ray scattering
          Density functional theory
          Simulation methods & models
      ab: The interaction of water with metal oxide surfaces plays a crucial role in the catalytic and geochemical behavior of metal oxides. In a vast majority of studies, the interfacial structure is assumed to arise from a relatively static lowest energy configuration of atoms, even at room temperature. Using hematite (α-FeO) as a model oxide, we show through a direct comparison of in situ synchrotron X-ray scattering with density functional theory-based molecular dynamics simulations that the structure of the (11-02) termination is dynamically stabilized by picosecond water exchange. Simulations show frequent exchanges between terminal aquo groups and adsorbed water in locations and with partial residence times consistent with experimentally determined atomic sites and fractional occupancies. Frequent water exchange occurs even for an ultrathin adsorbed water film persisting on the surface under a dry atmosphere. The resulting time-averaged interfacial structure consists of a ridged lateral arrangement of adsorbed water molecules hydrogen bonded to terminal aquo groups. Surface pK prediction based on bond valence analysis suggests that water exchange will influence the proton-transfer reactions underlying the acid/base reactivity at the interface. Our findings provide important new insights for understanding complex interfacial chemical processes at metal oxide-water interfaces.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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