Combined Homogeneous Surface Diffusion Model – Design of experiments approach to optimize dye adsorption considering both equilibrium and kinetic aspects.

Adsorption, a popular technique for removing azo dyes from aqueous streams, is influenced by several factors such as pH, initial dye concentration, temperature and adsorbent dosage. Any strategy that seeks to identify optimal conditions involving these factors, should take into account both kinetic...

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Publicado en:Journal of Environmental Management Vol. 204; pp. 424 - 436
Autores principales: Muthukkumaran, A., Aravamudan, K.
Formato: Artículo
Publicado: Academic Press Inc. Dec2017 Part 1
Materias:
Acceso en línea:Ver este registro en EBSCOhost
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      jtl: Journal of Environmental Management
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      dt: Dec2017 Part 1
      vid: 204
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      pub: Academic Press Inc.
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        125570060
        10.1016/j.jenvman.2017.09.010
      ppf: 424
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        atl: Combined Homogeneous Surface Diffusion Model – Design of experiments approach to optimize dye adsorption considering both equilibrium and kinetic aspects.
      aug:
        au:
          Muthukkumaran, A.
          Aravamudan, K.
        affil: Department of Chemical Engineering, Indian Institute of Technology Madras, Chennai, 600036, India
      su:
        Surface diffusion
        Azo dye testing
        Experimental design
        Adsorption capacity
        Structural optimization
      sug:
        subj:
          Surface diffusion
          Azo dye testing
          Experimental design
          Adsorption capacity
          Structural optimization
      keyword:
        Adsorption
        Azo-dye
        Central Composite Design (CCD)
        Design of experiments (DOE)
        Homogeneous Surface Diffusion Model (HSDM)
        Optimization
        Adsorption
        Azo-dye
        Central Composite Design (CCD)
        Design of experiments (DOE)
        Homogeneous Surface Diffusion Model (HSDM)
        Optimization
      ab: Adsorption, a popular technique for removing azo dyes from aqueous streams, is influenced by several factors such as pH, initial dye concentration, temperature and adsorbent dosage. Any strategy that seeks to identify optimal conditions involving these factors, should take into account both kinetic and equilibrium aspects since they influence rate and extent of removal by adsorption. Hence rigorous kinetics and accurate equilibrium models are required. In this work, the experimental investigations pertaining to adsorption of acid orange 10 dye (AO10) on activated carbon were carried out using Central Composite Design (CCD) strategy. The significant factors that affected adsorption were identified to be solution temperature, solution pH, adsorbent dosage and initial solution concentration. Thermodynamic analysis showed the endothermic nature of the dye adsorption process. The kinetics of adsorption has been rigorously modeled using the Homogeneous Surface Diffusion Model (HSDM) after incorporating the non-linear Freundlich adsorption isotherm. Optimization was performed for kinetic parameters (color removal time and surface diffusion coefficient) as well as the equilibrium affected response viz. percentage removal. Finally, the optimum conditions predicted were experimentally validated.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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