Evaluation of potential metabolomic-based biomarkers of protein, carbohydrate and fat intakes using a controlled feeding study.

Purpose: Objective biomarkers of dietary exposure are needed to establish reliable diet-disease associations. Unfortunately, robust biomarkers of macronutrient intakes are scarce. We aimed to assess the utility of serum, 24-h urine and spot urine high-dimensional metabolites for the development of b...

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Published in:European Journal of Nutrition Vol. 60; no. 8; pp. 4207 - 4219
Main Authors: Zheng, Cheng, Gowda, G. A. Nagana, Raftery, Daniel, Neuhouser, Marian L., Tinker, Lesley F., Prentice, Ross L., Beresford, Shirley A. A., Zhang, Yiwen, Bettcher, Lisa, Pepin, Robert, Djukovic, Danijel, Gu, Haiwei, Barding Jr., Gregory A., Song, Xiaoling, Lampe, Johanna W.
Format: research tables/charts Journal Article
Published: Springer Nature Dec2021
Online Access:View this record in EBSCOhost
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      jtl: European Journal of Nutrition
      issn: 14366207
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      dt: Dec2021
      vid: 60
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      pub: Springer Nature
      place: New York, New York
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        10.1007/s00394-021-02577-1
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        atl: Evaluation of potential metabolomic-based biomarkers of protein, carbohydrate and fat intakes using a controlled feeding study.
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        au:
          Zheng, Cheng
          Gowda, G. A. Nagana
          Raftery, Daniel
          Neuhouser, Marian L.
          Tinker, Lesley F.
          Prentice, Ross L.
          Beresford, Shirley A. A.
          Zhang, Yiwen
          Bettcher, Lisa
          Pepin, Robert
          Djukovic, Danijel
          Gu, Haiwei
          Barding Jr., Gregory A.
          Song, Xiaoling
          Lampe, Johanna W.
        affil: Department of Biostatistics, University of Nebraska Medical Center, Omaha, NE, USA
      sug:
        subj:
          Metabolomics
          Biological Markers Analysis
          Dietary Proteins Analysis
          Dietary Carbohydrates Analysis
          Dietary Fats Analysis
          Food Intake Evaluation
          Human
          Postmenopause
          Women
          Macronutrients Analysis
          Energy Intake
          Urinalysis
          Chromatography, Liquid
          Metabolites
          Magnetic Resonance Spectroscopy Methods
          Gas Chromatography-Mass Spectrometry Methods
          Correlation Coefficient
          Energy Density Evaluation
          Nutrition
      ab: Purpose: Objective biomarkers of dietary exposure are needed to establish reliable diet-disease associations. Unfortunately, robust biomarkers of macronutrient intakes are scarce. We aimed to assess the utility of serum, 24-h urine and spot urine high-dimensional metabolites for the development of biomarkers of daily intake of total energy, protein, carbohydrate and fat, and the percent of energy from these macronutrients (%E). Methods: A 2-week controlled feeding study mimicking the participants' habitual diets was conducted among 153 postmenopausal women from the Women's Health Initiative (WHI). Fasting serum metabolomic profiles were analyzed using a targeted liquid chromatography–tandem mass spectrometry (LC–MS/MS) assay for aqueous metabolites and a direct-injection-based quantitative lipidomics platform. Urinary metabolites were analyzed using 1H nuclear magnetic resonance (NMR) spectroscopy at 800 MHz and by untargeted gas chromatography–mass spectrometry (GC–MS). Variable selection was performed to build prediction models for each dietary variable. Results: The highest cross-validated multiple correlation coefficients (CV-R2) for protein intake (%E) and carbohydrate intake (%E) using metabolites only were 36.3 and 37.1%, respectively. With the addition of established dietary biomarkers (doubly labeled water for energy and urinary nitrogen for protein), the CV-R2 reached 55.5% for energy (kcal/d), 52.0 and 45.0% for protein (g/d, %E), 55.9 and 37.0% for carbohydrate (g/d, %E). Conclusion: Selected panels of serum and urine metabolites, without the inclusion of doubly labeled water and urinary nitrogen biomarkers, give a reliable and robust prediction of daily intake of energy from protein and carbohydrate.
      pubtype: Academic Journal
      doctype:
        research
        tables/charts
        Journal Article
      ougenre: Article
    language: English
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