Removal of Methyl Violet from Aqueous solutions using Sr2ANbO5.5 (A= Ca+2, Sr+2 & Ba+2).

Three members of the A-site doped Nb perovskites with general formula Sr2CaNbO5.5, Sr3NbO5.5 and BaSr2NbO5.5 were synthesised by solid-state methods and their removal efficiency of Methyl violet from aqueous solutions investigated. The X-ray diffraction measurements demonstrated that the three sampl...

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Publicado en:Revista CENIC Ciencias Quimicas no. 1; pp. 1 - 13
Autores principales: Alnaas, Maryam M., Awin, Labib A., El-Rais, Mahmoud A., Etorki, Abdunnaser M., Ezrgane, Moda M.
Formato: Artículo
Publicado: Centro Nacional de Investigaciones Cientificas ene-jun2022
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Acceso en línea:Ver este registro en EBSCOhost
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        atl: Removal of Methyl Violet from Aqueous solutions using Sr2ANbO5.5 (A= Ca+2, Sr+2 & Ba+2).
      aug:
        au:
          Alnaas, Maryam M.
          Awin, Labib A.
          El-Rais, Mahmoud A.
          Etorki, Abdunnaser M.
          Ezrgane, Moda M.
        affil:
          Chemistry Department, Faculty of Science, Gharyan University, Libya
          Chemistry Department, Faculty of Science, Tripoli University, Libya
      su:
        Gentian violet
        Alkaline earth metals
        Aqueous solutions
        X-ray diffraction
        Perovskite
        X-ray diffraction measurement
        Adsorption (Chemistry)
        Space groups
        Basic dyes
        Cell size
        Sorbents
        Nanoparticles
      sug:
        subj:
          Gentian violet
          Alkaline earth metals
          Aqueous solutions
          X-ray diffraction
          Perovskite
          X-ray diffraction measurement
          Adsorption (Chemistry)
          Space groups
          Basic dyes
          Cell size
          Sorbents
          Nanoparticles
      keyword:
        A-site Doping
        Methyl violet
        Removal
        dopaje en el sitio A
        Eliminación
        violeta de metilo
      ab:
        Three members of the A-site doped Nb perovskites with general formula Sr2CaNbO5.5, Sr3NbO5.5 and BaSr2NbO5.5 were synthesised by solid-state methods and their removal efficiency of Methyl violet from aqueous solutions investigated. The X-ray diffraction measurements demonstrated that the three samples have a faced cubic perovskite-type structure in space group Fm m. The additions of Ba2+ and Ca2+ into the A-site of Sr3NbO5.5 have influenced the cell volume, crystal size and density. Subsequently, the removal capacity was also impacted. The crystallite size of the three oxides was calculated to be less than 82 nm. The maximum removal capacities of Methyl violet are found to be 46.5, 13.1 and 8.0 mg/g using BaSr2NbO5.5, Sr3NbO5.5 and CaSr2NbO5.5, respectively. The amounts of the adsorbed dye have decreased as the ionic radii of the doped decreased. The removals of Methyl violet have a positive relationship with pH, temperature and the mass of the oxides.
        Tres miembros de las perovskitas de Nb dopadas en el sitio A con la fórmula general Sr2CaNbO5.5, Sr3NbO5.5 y BaSr2NbO5.5 se sintetizaron mediante métodos de estado sólido y se investigó su eficiencia de eliminación de violeta de metilo de soluciones acuosas. Las mediciones de difracción de rayos X demostraron que las tres muestras tienen una estructura de tipo perovskita cúbica enfrentada en el grupo espacial Fm3 ̅m. Las adiciones de Ba2+ y Ca2+ en el sitio A de Sr3NbO5.5 han influido en el volumen celular, el tamaño del cristal y la densidad. Posteriormente, la capacidad de remoción también se vio afectada. Se calculó que el tamaño de los cristalitos de los tres óxidos era inferior a 82 nm. Las capacidades máximas de eliminación de violeta de metilo son de 46,5, 13,1 y 8,0 mg/g utilizando BaSr2NbO5,5, Sr3NbO5,5 y CaSr2NbO5,5, respectivamente. Las cantidades del colorante adsorbido han disminuido a medida que disminuían los radios iónicos del dopado. Las remociones de violeta de metilo tienen una relación positiva con el pH, la temperatura y la masa de los óxidos.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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      holder: Centro Nacional de Investigaciones Cientificas
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          year: 2022
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