Characterization of Oxygen Dynamics in ZrWO.

The dynamics of oxygen motion in ZrWO have been characterized using O solid-state NMR. Rates of dynamic exchange have been extracted from magnetization transfer experiments over a temperature range of 40 to 226 °C, and distinct values for the associated activation barrier have been observed on eithe...

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Publicado en:Journal of the American Chemical Society Vol. 127; no. 43; pp. 15175 - 15182
Autores principales: Hampson, Matthew R., Evans, John S. O., Hodgkinson, Paul
Formato: Artículo
Publicado: American Chemical Society 11/2/2005
Materias:
Acceso en línea:Ver este registro en EBSCOhost
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      aug:
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          Hampson, Matthew R.
          Evans, John S. O.
          Hodgkinson, Paul
        affil: Department of Chemistry, Durham University, South Road, Durham DH1 3LE, United Kingdom.
      su:
        Ferromagnetism
        Photosynthetic oxygen evolution
        Magnetization
        Optical diffraction
        Magnetism
        Oxygen
      sug:
        subj:
          Ferromagnetism
          Photosynthetic oxygen evolution
          Magnetization
          Optical diffraction
          Magnetism
          Oxygen
      ab: The dynamics of oxygen motion in ZrWO have been characterized using O solid-state NMR. Rates of dynamic exchange have been extracted from magnetization transfer experiments over a temperature range of 40 to 226 °C, and distinct values for the associated activation barrier have been observed on either side of the order/disorder phase transition at ∼1 75°C. A detailed model for the dynamical process is proposed, which reconciles the observation of continuing oxygen dynamics in the low-temperature phase with the static order implied by earlier X-ray diffraction studies.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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