Mechanistic insights into Helicobacter pylori urease inhibition by poplar propolis ethanol extract.

Propolis, a resinous mixture from plant exudates, is widely used in traditional ethnomedicine for gastrointestinal infections, implying anti- Helicobacter pylori (H. pylori) potential. However, its molecular mechanisms targeting H. pylori urease (HPU), a key virulence factor, remain unclear. This st...

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Publicado en:Journal of Ethnopharmacology Vol. 365
Autores principales: Yuan, Jie, Li, Ting, Gao, Shuangshuang, Tang, Yujing, Ma, Shuling, Lee, Hai Yen, Chin, Kim Ling, Xuan, Hongzhuan
Formato: research Journal Article
Publicado: Elsevier B.V. Jun2026
Acceso en línea:Ver este registro en EBSCOhost
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      issn: 03788741
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      dt: Jun2026
      vid: 365
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      pub: Elsevier B.V.
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        10.1016/j.jep.2026.121596
        192840445
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        atl: Mechanistic insights into Helicobacter pylori urease inhibition by poplar propolis ethanol extract.
      aug:
        au:
          Yuan, Jie
          Li, Ting
          Gao, Shuangshuang
          Tang, Yujing
          Ma, Shuling
          Lee, Hai Yen
          Chin, Kim Ling
          Xuan, Hongzhuan
        affil: College of Agriculture and Biology, Liaocheng University, Liaocheng, People's Republic of China
      sug:
        subj:
          Helicobacter Pylori
          Urease
          Enzyme Inhibitors
          Propolis Therapeutic Use
          Gastrointestinal Diseases
          Plant Extracts Pharmacodynamics
          Ethanol Pharmacodynamics
          Medicine, Herbal
          Human
          Kinetics
          Antibiotics Therapeutic Use
          Flavonoids
          Phenols
      ab: Propolis, a resinous mixture from plant exudates, is widely used in traditional ethnomedicine for gastrointestinal infections, implying anti- Helicobacter pylori (H. pylori) potential. However, its molecular mechanisms targeting H. pylori urease (HPU), a key virulence factor, remain unclear. This study aimed to characterize the inhibitory activity and kinetic properties of poplar propolis ethanol extract (PPEE) against HPU and jack bean urease (JBU), and to elucidate the underlying molecular mechanisms. UPLC–MS/MS-based metabolomics was used to identify PPEE's potential bioactive candidates. Enzyme activity assays, kinetic analysis, thiol/Ni2+ protection assays, transcriptional profiling of urease-related genes, and molecular docking were applied for mechanistic exploration. Bacterial growth curve assays and PI staining verified its antibacterial activity. PPEE, enriched in flavonoids and phenolic acids, exhibited significant dose-dependent and reversible inhibition on HPU, with superior potency to JBU. Mechanistically, PPEE acted synergistically by competitively binding to HPU's substrate pocket, disrupting thiol-Ni2+ coordination, inducing slow-binding conformational stabilization, and perturbing tertiary structure. It also downregulated ureA / ureB , nixA , and ureH / ureI , forming a multi-layered mode of "direct enzyme inhibition + blocking synthesis/assembly". Urease inhibition was the core anti- H. pylori mechanism, with auxiliary urease-independent activity. Molecular docking confirmed stable interactions between PPEE components and HPU's active center/substrate pocket. Experimental validation showed that quercetin and taxifolin inhibited HPU in a dose-dependent manner. PPEE specifically inhibits HPU via multi-targeted synergistic mechanisms, providing molecular evidence for propolis-derived anti- H. pylori agents and laying a foundation for subsequent SAR and in vivo studies. Poplar propolis ethanol extract (PPEE) inhibits Helicobacter pylori (H. pylori) through multi-target urease modulation. PPEE competitively inhibits H. pylori urease (HPU), targets thiol groups for reversible inhibition, disrupts urease tertiary structure, and downregulates urease-related genes, thereby blocking enzyme assembly. These combined effects result in antibacterial activity via both urease-dependent and auxiliary urease-independent mechanisms. [Display omitted]
      pubtype: Academic Journal
      doctype:
        research
        Journal Article
      ougenre: Article
    language: English
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