Theoretical Studies of Quantum Amplified Isomerizations for Imaging Systems Involving Hexamethyl Dewar Benzene and Related Systems.

The ring-opening reactions of the radical cations of hexamethyl Dewar benzene (1) and Dewar benzene have been studied using density functional theory (DFT) and complete active-space self-consistent field (CASSCF) calculations. Compound 1 is known to undergo photoinitiated ring opening by a radical c...

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Publicado en:Journal of the American Chemical Society Vol. 128; no. 24; pp. 7835 - 7846
Autores principales: Norton, Joseph E., Olson, Leif P., Houk, K. N.
Formato: Artículo
Publicado: American Chemical Society 6/21/2006
Materias:
Acceso en línea:Ver este registro en EBSCOhost
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        10.1021/ja060182i
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        atl: Theoretical Studies of Quantum Amplified Isomerizations for Imaging Systems Involving Hexamethyl Dewar Benzene and Related Systems.
      aug:
        au:
          Norton, Joseph E.
          Olson, Leif P.
          Houk, K. N.
        affil:
          Department of Chemistry and Biochemistry, University of California, Los Angeles, California 90095-1569
          Research & Development, Eastman Kodak Company, Rochester, New York 14650-2109
      su:
        Ring-opening polymerization
        Isomerization
        Benzene
        Imaging systems
        Density functionals
        Cations
        Quantum chemistry
      sug:
        subj:
          Ring-opening polymerization
          Isomerization
          Benzene
          Imaging systems
          Density functionals
          Cations
          Quantum chemistry
      ab: The ring-opening reactions of the radical cations of hexamethyl Dewar benzene (1) and Dewar benzene have been studied using density functional theory (DFT) and complete active-space self-consistent field (CASSCF) calculations. Compound 1 is known to undergo photoinitiated ring opening by a radical cation chain mechanism, termed ‘quantum amplified isomerization’ (QAI), which is due to the high quantum yield. Why QAI is efficient for 1 but not other reactions is explained computationally. Two radical cation minima of 1 and transition states located near avoided crossings are identified. The state crossings are characterized by conical intersections corresponding to degeneracy between doublet surfaces. Ring opening occurs by formation of the radical cation followed by a decrease in the flap dihedral angle. A rate-limiting C transition state leads to a second stable radical cation with an elongated transannular CC bond and an increased flap dihedral. This structure proceeds through a conrotatory-like pathway of C symmetry to give the benzene radical cation. The role of electron transfer was investigated by evaluating oxidation of various systems using adiabatic ionization energies and electron affinities calculated from neutral and cation geometries. Electron-transfer theory was applied to 1 to investigate the limiting effects of back-electron transfer as it is related to the unusual stability of the two radical cations. Expected changes in optical properties between reactants and products of Dewar benzene compounds and other systems known to undergo QAI were characterized by computing frequency-dependent indices of refraction from isotropic polarizabilities. In particular, the reaction of 1 shows greater contrast in index of refraction than that of the Dewar benzene parent system.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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