Stern-Gerlach Experiments of One-Dimensional Metal-Benzene Sandwich Clusters: M(CH) (M = Al, Sc, Ti, and V).

A molecular beam of multilayer metal-benzene organometallic clusters M(CH) (M = Al, Sc, Ti, and V) was produced by a laser vaporization synthesis method, and their magnetic deflections were measured. Multidecker sandwich clusters of transition-metal atoms and benzene Sc(CH) (n = 1, 2) and V(CH) (n =...

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Publicado en:Journal of the American Chemical Society Vol. 129; no. 27; pp. 8473 - 8481
Autores principales: Miyajima, Ken, Yabushita, Satoshi, Knickelbein, Mark B., Nakajima, Atsushi
Formato: Artículo
Publicado: American Chemical Society 7/11/2007
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Acceso en línea:Ver este registro en EBSCOhost
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      dt: 7/11/2007
      vid: 129
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      pub: American Chemical Society
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        atl: Stern-Gerlach Experiments of One-Dimensional Metal-Benzene Sandwich Clusters: M(CH) (M = Al, Sc, Ti, and V).
      aug:
        au:
          Miyajima, Ken
          Yabushita, Satoshi
          Knickelbein, Mark B.
          Nakajima, Atsushi
        affil:
          Department of Chemistry, Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama 223-8522, Japan
          Chemistry Division and Center for Nanoscale Materials, Argonne National Laboratory, Argonne, Illinois 60439
          CREST, Japan Science and Technology Agency (JST), c/o Department of Chemistry, Keio University, Yokohama 223-8522, Japan
      su:
        Organometallic compounds
        Molecular beams
        Benzene
        Metal clusters
        Microclusters
        Relaxation phenomena
        Magnetism
      sug:
        subj:
          Organometallic compounds
          Molecular beams
          Benzene
          Metal clusters
          Microclusters
          Relaxation phenomena
          Magnetism
      ab: A molecular beam of multilayer metal-benzene organometallic clusters M(CH) (M = Al, Sc, Ti, and V) was produced by a laser vaporization synthesis method, and their magnetic deflections were measured. Multidecker sandwich clusters of transition-metal atoms and benzene Sc(CH) (n = 1, 2) and V(CH) (n = 1-4) possess magnetic moments that increase monotonously with n. The magnetic moments of AI(CH), Sc(CH), and V(CH) are smaller than that of their spin-only values as a result of intracluster spin relaxation, an effect that depends on the orbital angular momenta and bonding characters of the orbitals containing electron spin. While Ti(CH) was found to be nonmagnetic, Ti(CH) (n = 2, 3) possess nonzero magnetic moments. The mechanism of ferromagnetic spin ordering in M-(CH) (M = Sc, Ti, V) is discussed qualitatively in terms of molecular orbital analysis. These sandwich species represent a new class of one-dimensional molecular magnets in which the transition-metal atoms are formally zerovalent.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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          year: 2007
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