Free-Standing Nanocomposite Multilayers with Various Length Scales, Adjustable Internal Structures, and Functionalities.

We introduce an innovative and robust method for the preparation of nanocomposite multilayers, which allows accurate control over the placement of functional groups as well as the composition and dimensions of individual layers/internal structure. By employing the photocross-linkable polystyrene (PS...

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Publicado en:Journal of the American Chemical Society Vol. 131; no. 7; pp. 2579 - 2588
Autores principales: Lee, Seryun, Lee, Bokyoung, Kim, Bumjoon J., Park, Junwoo, Yoo, Misang, Bae, Wan Ki, Char, Kookheon, Hawker, Craig J., Bang, Joona, Cho, Jinhan
Formato: Artículo
Publicado: American Chemical Society 2/25/2009
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Acceso en línea:Ver este registro en EBSCOhost
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      dt: 2/25/2009
      vid: 131
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      pub: American Chemical Society
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        37143983
        10.1021/ja8064478
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        atl: Free-Standing Nanocomposite Multilayers with Various Length Scales, Adjustable Internal Structures, and Functionalities.
      aug:
        au:
          Lee, Seryun
          Lee, Bokyoung
          Kim, Bumjoon J.
          Park, Junwoo
          Yoo, Misang
          Bae, Wan Ki
          Char, Kookheon
          Hawker, Craig J.
          Bang, Joona
          Cho, Jinhan
        affil:
          School of Advanced Materials Engineering, Kookmin University, Jeongneung-dong, Seongbuk-gu, Seoul 136-702, Korea
          Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology, Daejeon 305-701, Korea
          Department of Chemical and Biological Engineering, Korea University, Anam-dong, Seongbuk-gu, Seoul 136-701, Korea
          School of Chemical and Biological Engineering, Seoul National University, San 56-1, Shinlim-dong, Kwanak-gu, Seoul 151-744, Korea
          Materials Research Laboratory, University of California, Santa Barbara, California 93106-5121
      su:
        Nanostructures
        Composite materials
        Photoluminescence
        Functional groups
        Crosslinked polymers
      sug:
        subj:
          Nanostructures
          Composite materials
          Photoluminescence
          Functional groups
          Crosslinked polymers
      ab: We introduce an innovative and robust method for the preparation of nanocomposite multilayers, which allows accurate control over the placement of functional groups as well as the composition and dimensions of individual layers/internal structure. By employing the photocross-linkable polystyrene (PS-N, M = 28.0 kg/mol) with 10 wt % azide groups (-N) for host polymer and/or the PS-N3-SH (M = 6.5 kg/mol) with azide and thiol (-SH) groups for capping ligands of inorganic nanoparticles, nanocomposite multilayers were prepared by an efficient photocross-linking layer-by-layer process, without perturbing underlying layers and nanostructures. The thickness of individual layers could be controlled from a few to hundreds of nanometers producing highly ordered internal structure, and the resulting nanocomposite multilayers, consisting of polymer and inorganic nanoparticles (CdSe@ZnS, Au, and Pt), exhibit a variety of interesting physical properties. These include prolonged photoluminescent durability, facile color tuning, and the ability to prepare functional free-standing films that can have the one-dimensional photonic band gap and furthermore be patterned by photolithography. This robust and tailored method opens a new route for the design of functional film devices based on nanocomposite multilayers.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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          year: 2009
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