Origin of Photocatalytic Activity of Nitrogen-Doped TiO Nanobelts.

Experiments combined with the density functional theory (DFT) calculation have been performed to understand the underlying photocatalysis mechanism of the nitrogen-doped titania nanobelts. Nitrogen-doped anatase titania nanobelts are prepared via hydrothermal processing and subsequent heat treatment...

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Published in:Journal of the American Chemical Society Vol. 131; no. 34; pp. 12290 - 12298
Main Authors: Jin Wang, De Nyago Tafen, Lewis, James P., Zhanglian Hong, Manivannan, Ayyakkannu, Mingjia Zhi, Ming Li, Nianqiang Wu
Format: Article
Published: American Chemical Society 9/2/2009
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Online Access:View this record in EBSCOhost
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      dt: 9/2/2009
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      pub: American Chemical Society
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        10.1021/ja903781h
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        atl: Origin of Photocatalytic Activity of Nitrogen-Doped TiO Nanobelts.
      aug:
        au:
          Jin Wang
          De Nyago Tafen
          Lewis, James P.
          Zhanglian Hong
          Manivannan, Ayyakkannu
          Mingjia Zhi
          Ming Li
          Nianqiang Wu
        affil:
          Department of Mechanical and Aerospace Engineering, WVNano Initiative, West Virginia University, Morgantown, West Virginia 26506-6106
          Department of Physics, West Virginia University, Morgantown, West Virginia 26506
          State Key Laboratory of Silicon Materials, Department of Materials Science & Engineering, Zhejiang University, Hangzhou 310027, P.R. China
          National Energy Technology Laboratory, U.S. Department of Energy, Morgantown, West Virginia 26507
      su:
        Molecular spectroscopy
        Photoelectron spectroscopy
        Molecular orbitals
        Density functionals
        Electron spectroscopy
        Dislocations in crystals
      sug:
        subj:
          Molecular spectroscopy
          Photoelectron spectroscopy
          Molecular orbitals
          Density functionals
          Electron spectroscopy
          Dislocations in crystals
      ab: Experiments combined with the density functional theory (DFT) calculation have been performed to understand the underlying photocatalysis mechanism of the nitrogen-doped titania nanobelts. Nitrogen-doped anatase titania nanobelts are prepared via hydrothermal processing and subsequent heat treatment in NH. Both the nitrogen content and the oxygen vacancy concentration increase with increasing the NH treatment temperature. Nitrogen doping leads to an add-on shoulder on the edge of the valence band, the localized N 2p levels above the valence band maximum, and the 3d states of Ti below the conduction band, which is confirmed by DFT calculation and X-ray photoelectron spectroscopy (XPS) measurement. Extension of the light absorption from the ultraviolet (UV) region to the visible-light region arises from the N 2p levels near the valence band and from the color centers induced by the oxygen vacancies and the Ti species. Nitrogen doping allows visible-light-responsive photocatalytic activity but lowers UV-light-responsive photocatalytic activity. The visible-light photocatalytic activity originates from the N 2p levels near the valence band. The oxygen vacancies and the associated Ti species act as the recombination centers for the photoinduced electrons and holes. They reduce the photocatalytic activity although they contribute to the visible light absorbance.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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