Ligand-assisted degradation of carbon tetrachloride by microscale zero-valent iron

Degradation of carbon tetrachloride (CT) by microscale zero-valent iron (ZVI) was investigated in batch systems with or without organic ligands (ethylenediaminetetraacetic acid (EDTA), citric acid, tartaric acid, malic acid and oxalic acid) at pHs from 3.5 to 7.5. The results demonstrated that at 25...

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Publicado en:Journal of Environmental Management Vol. 92; no. 4; pp. 1328 - 1334
Autores principales: Zhang, Xianlan, Deng, Baolin, Guo, Jing, Wang, Yang, Lan, Yeqing
Formato: Artículo
Publicado: Academic Press Inc. Apr2011
Materias:
Acceso en línea:Ver este registro en EBSCOhost
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      dt: Apr2011
      vid: 92
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      pub: Academic Press Inc.
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        57689983
        10.1016/j.jenvman.2010.12.020
      ppf: 1328
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        atl: Ligand-assisted degradation of carbon tetrachloride by microscale zero-valent iron
      aug:
        au:
          Zhang, Xianlan
          Deng, Baolin
          Guo, Jing
          Wang, Yang
          Lan, Yeqing
        affil:
          College of Sciences, Nanjing Agricultural University, Nanjing 210095, PR China
          Department of Civil and Environmental Engineering, University of Missouri, Columbia, MO 65211, USA
      su:
        Environmental engineering
        Carbon tetrachloride
        Industrial waste purification
        Environmental chemistry
        Iron & the environment
        Ligands (Chemistry)
        Ethylenediaminetetraacetic acid
        Batch processing
        pH effect
      sug:
        subj:
          Environmental engineering
          Other basic organic chemical manufacturing
          All Other Basic Organic Chemical Manufacturing
          Metal service centres
          Iron and Steel Mills and Ferroalloy Manufacturing
          Carbon tetrachloride
          Industrial waste purification
          Environmental chemistry
          Iron & the environment
          Ligands (Chemistry)
          Ethylenediaminetetraacetic acid
          Batch processing
          pH effect
      keyword:
        Dechlorination
        Organic ligands
        Zero-valent iron
        Dechlorination
        Organic ligands
        Zero-valent iron
      ab: Degradation of carbon tetrachloride (CT) by microscale zero-valent iron (ZVI) was investigated in batch systems with or without organic ligands (ethylenediaminetetraacetic acid (EDTA), citric acid, tartaric acid, malic acid and oxalic acid) at pHs from 3.5 to 7.5. The results demonstrated that at 25°C, the dechlorination of CT by microscale ZVI is slow in the absence of organic ligands, with a pseudo-first-order rate constant of 0.0217h at pH 3.5 and being further dropped to 0.0052h at pH 7.5. However, addition of organic ligands significantly enhanced the rates and the extents of CT removal, as indicated by the rate constant increases of 39, 31, 32, 28 and 18 times in the presence of EDTA, citric acid, tartaric acid, malic acid and oxalic acid, respectively, at pH 3.5 and 25°C. The effect of EDTA was most significant; the dechlorination of CT at an initial concentration of 20mgl increased from 16.3% (no ligands) to 89.1% (with EDTA) at the end of 8h reaction. The enhanced CT degradation in the presence of organic ligands was primarily attributed to the elimination of a surface passivation layer of Fe(III) (hydr)oxides on the microscale ZVI through chelating of organic ligands with Fe(III), which maintained the exposure of active sites on ZVI surface to CT.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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