Anion Modules: Building Blocks of Supramolecular Assemblies by Combination with π-Conjugated Anion Receptors.

Dipyrrolyldiketone boron complexes, as π-conjugated acyclic anion receptors, act as building sub-units of various assemblies through noncovalent interactions in the form of receptor-anion complexes. Instead of, or in addition to, the modffication of receptor structures, the introduction of anion mod...

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Publicado en:Journal of the American Chemical Society Vol. 133; no. 23; pp. 8896 - 8900
Autores principales: Maeda, Hiromitsu, Naritani, Kazumasa, Honsho, Yoshihito, Shu Seki
Formato: Artículo
Publicado: American Chemical Society 6/15/2011
Materias:
Acceso en línea:Ver este registro en EBSCOhost
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      dt: 6/15/2011
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      pub: American Chemical Society
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        10.1021/ja203880d
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        atl: Anion Modules: Building Blocks of Supramolecular Assemblies by Combination with π-Conjugated Anion Receptors.
      aug:
        au:
          Maeda, Hiromitsu
          Naritani, Kazumasa
          Honsho, Yoshihito
          Shu Seki
        affil:
          College of Pharmaceutical Sciences, Institute of Science and Engineering, Ritsumeikan University, Kusatsu 525-8577, Japan
          Department of Applied Chemistry, Graduate School of Engineering, Osaka University, Suita 565-0871, Japan
          PRESTO, Japan Science and Technology Agency (JST), Kawaguchi 332-0012, Japan
      su:
        Boron compounds
        Anions
        X-ray diffraction
        Calorimetry
        Electric conductivity
        Microscopy
      sug:
        subj:
          Boron compounds
          Anions
          X-ray diffraction
          Calorimetry
          Electric conductivity
          Microscopy
      ab: Dipyrrolyldiketone boron complexes, as π-conjugated acyclic anion receptors, act as building sub-units of various assemblies through noncovalent interactions in the form of receptor-anion complexes. Instead of, or in addition to, the modffication of receptor structures, the introduction of anion modules as building blocks for the assemblies was found to be useful in forming various soft materials. Gallic carboxylate derivatives 3-n (n = 16, 18, 20), as tetrabutylammonium (TBA) salts, form receptor-anion-module complexes that can be used to fabricate supramolecular assemblies. Combinations of aliphatic anion modules 3-n and receptors 1a,b along with a TBA cation afforded products with mesophases, which were indicated by differential scanning calorimetry and polarized optical microscopy. X-ray diffraction measurements of the solid states and mesophases of 1a·3-n·TBA and 1b·3-n·TBA revealed highly ordered structures including lamellar structures, which could be modulated by the lengths of the alkyl chains of the modules. Functional materials exhibiting electrical conductivity were fabricated by using combinations of anionic building blocks that form assemblies by themselves and π-conjugated acydic receptors.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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          year: 2011
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