Ultrafast and Continuous Synthesis of Unaccommodating Inorganic Nanomaterials in Droplet- and Ionic Liquid-Assisted Microfluidic System.
Despite many efforts on the synthesis of inorganic nanomaterials with uniform structure and narrow size distribution in a fast and continuous way, it is still a critical challenge in the chemistry research community due to the uncontrollable mass and heat transfer and the harsh experimental conditio...
| Publicado en: | Journal of the American Chemical Society Vol. 133; no. 37; pp. 14765 - 14771 |
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| Autores principales: | , , |
| Formato: | Artículo |
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American Chemical Society
9/21/2011
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| Acceso en línea: | Ver este registro en EBSCOhost |
| fields | @attributes: recordID: 1 pdfLink: plink: https://search.ebscohost.com/login.aspx?direct=true&db=hlh&AN=66701890&site=ehost-live header: @attributes: shortDbName: hlh uiTerm: 66701890 longDbName: Humanities International Complete uiTag: AN controlInfo: bkinfo: jinfo: jid: 00027863 ACS jtl: Journal of the American Chemical Society issn: 00027863 maglogo: N pubinfo: dt: 9/21/2011 vid: 133 iid: 37 pid: 997 pub: American Chemical Society artinfo: ui: 66701890 10.1021/ja2054429 ppf: 14765 ppct: 6 formats: tig: atl: Ultrafast and Continuous Synthesis of Unaccommodating Inorganic Nanomaterials in Droplet- and Ionic Liquid-Assisted Microfluidic System. aug: au: Phan Huy Hoang HoSeok Park Dong-Pyo Kim affil: National Creative Research Center of Applied Microfluidic Chemistry, Chungnam National University, Daejeon 305-764, South Korea Department of Chemical Engineering, College of Engineering, KyungHee University, 1 Seochon-dong, Giheung-gu, Youngin-si, Gyeonggi-do 446-701, Korea Graduate School of Analytical Science and Technology, Chungnam National University, Daejeon 305-764, South Korea su: Nanostructured materials Ionic liquids Microfluidics Uniform spaces Microreactors Microfluidic analytical techniques sug: subj: Nanostructured materials Ionic liquids Microfluidics Uniform spaces Microreactors Microfluidic analytical techniques ab: Despite many efforts on the synthesis of inorganic nanomaterials with uniform structure and narrow size distribution in a fast and continuous way, it is still a critical challenge in the chemistry research community due to the uncontrollable mass and heat transfer and the harsh experimental conditions of high temperature and pressure. Here we report a droplet- and ionic liquid-assisted microfluidic (DIM) synthesis method, which takes full advantage of both ionic liquids and droplet-assisted microreaction systems, for an ultrafast, mild, and continuous synthesis of various inorganic nanomaterials that takes only tens of minutes rather than days that are usually needed to synthesize. In particular, unaccommodating inorganic nanomaterials that are difficult to produce, such as nanoporous ZSM-5, γ-AlOOH, and β-FeOOH nanorods, were synthesized in only "20 minutes" of reaction time even with simple instrument. The DIM method delineated herein would offer a breakthrough synthetic approach for functional but unaccommodating inorganic nanomaterials in a continuous and mild manner. pubtype: Academic Journal doctype: Article src: R language: English refInfo: copyright: @attributes: flag: Y dt: @attributes: year: 2011 holdings: @attributes: islocal: N |
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