Mechanism of Ti-Catalyzed Oxidative Nitrene Transfer in [2 + 2 + 1] Pyrrole Synthesis from Alkynes and Azobenzene.

A combined computational and experimental study on the mechanism of Ti-catalyzed formal [2 + 2 + 1] pyrrole synthesis from alkynes and aryl diazenes is reported. This reaction proceeds through a formally Ti/Ti redox catalytic cycle as determined by natural bond orbital (NBO) and intrinsic bond orbit...

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Publicado en:Journal of the American Chemical Society Vol. 140; no. 23; pp. 7267 - 7282
Autores principales: Davis-Gilbert, Zachary W., Xuelan Wen, Goodpaster, Jason D., Tonks, Ian A.
Formato: Artículo
Publicado: American Chemical Society 6/13/2018
Acceso en línea:Ver este registro en EBSCOhost