Synthesis of Mixed-Valent Manganese Oxide Nanocrystals: An In situ Synchrotron X-ray Diffraction Study.

The article illustrates the characterizations of phase transformations by in situ synchrotron powder X-ray diffraction at different pH media. The in situ synchrotron X-ray diffraction studies provide an opportunity for better control of material syntheses. Furthermore, oxygen/cation vacancies or def...

Descripción completa

Detalles Bibliográficos
Publicado en:Journal of the American Chemical Society Vol. 128; no. 14; pp. 4570 - 4572
Autores principales: Xiong-Fei Shen, Yun-Shuang Ding, Hanson, Jonathan C., Aindow, Mark, Suib, Steven L.
Formato: Artículo
Publicado: American Chemical Society 4/12/2006
Materias:
Acceso en línea:Ver este registro en EBSCOhost
fields @attributes:
  recordID: 1
pdfLink:
plink: https://search.ebscohost.com/login.aspx?direct=true&db=hlh&AN=20780160&site=ehost-live
header:
  @attributes:
    shortDbName: hlh
    uiTerm: 20780160
    longDbName: Humanities International Complete
    uiTag: AN
  controlInfo:
    bkinfo:
    jinfo:
      jid:
        00027863
        ACS
      jtl: Journal of the American Chemical Society
      issn: 00027863
      maglogo: N
    pubinfo:
      dt: 4/12/2006
      vid: 128
      iid: 14
      pid: 997
      pub: American Chemical Society
    artinfo:
      ui:
        20780160
        10.1021/ja058456+
      ppf: 4570
      ppct: 2
      formats:
      tig:
        atl: Synthesis of Mixed-Valent Manganese Oxide Nanocrystals: An In situ Synchrotron X-ray Diffraction Study.
      aug:
        au:
          Xiong-Fei Shen
          Yun-Shuang Ding
          Hanson, Jonathan C.
          Aindow, Mark
          Suib, Steven L.
        affil:
          Institute of Materials Science, University of Connecticut, 55 North Eagleville Road, Storrs, Connecticut 06269
          Department of Chemistry, Brookhaven National Laboratory, Upton, New York 11973
          Department of Chemistry, University of Connecticut, 55 North Eagleville Road, Storrs, Connecticut 06269
          Department of Chemical Engineering, University of Connecticut, 55 North Eagleville Road, Storrs, Connecticut 06269
      su:
        Nanocrystals
        X-ray diffraction
        Synchrotrons
        Optical diffraction
        Chemistry
      sug:
        subj:
          Nanocrystals
          X-ray diffraction
          Synchrotrons
          Optical diffraction
          Chemistry
      ab: The article illustrates the characterizations of phase transformations by in situ synchrotron powder X-ray diffraction at different pH media. The in situ synchrotron X-ray diffraction studies provide an opportunity for better control of material syntheses. Furthermore, oxygen/cation vacancies or defects, combined with Rietveld refinement, can be studied to better understand the catalytic mechanism.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
    refInfo:
    copyright:
      @attributes:
        flag: Y
      dt:
        @attributes:
          year: 2006
    holdings:
      @attributes:
        islocal: N