Selective Detection and Inhibition of Active Caspase-3 in Cells with Optimized Peptides.

Caspases are a family of cysteine-aspartyl proteases that are well recognized for their essential roles in apoptosis and inflammation. Recently, caspases have also been linked to the promotion of other biologically important phenomena, such as cellular differentiation and proliferation. Dysregulatio...

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Publicado en:Journal of the American Chemical Society Vol. 135; no. 34; pp. 12869 - 12877
Autores principales: Vickers, Chris J., González-Páez, Gonzalo E., Wolan, Dennis W.
Formato: Artículo
Publicado: American Chemical Society 8/28/2013
Materias:
Acceso en línea:Ver este registro en EBSCOhost
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      dt: 8/28/2013
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      pub: American Chemical Society
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        10.1021/ja406399r
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        atl: Selective Detection and Inhibition of Active Caspase-3 in Cells with Optimized Peptides.
      aug:
        au:
          Vickers, Chris J.
          González-Páez, Gonzalo E.
          Wolan, Dennis W.
        affil: Departments of Molecular and Experimental Medicine and Chemical Physiology, The Scripps Research Institute, 10550 North Torrey Pines Road, La Jolla, California 92037, United States
      su:
        Caspases regulation
        Molecular probes
        Enzyme inhibitors
        Peptides
        Structural optimization
        Membrane permeability (Biology)
      sug:
        subj:
          Caspases regulation
          Molecular probes
          Enzyme inhibitors
          Peptides
          Structural optimization
          Membrane permeability (Biology)
      ab: Caspases are a family of cysteine-aspartyl proteases that are well recognized for their essential roles in apoptosis and inflammation. Recently, caspases have also been linked to the promotion of other biologically important phenomena, such as cellular differentiation and proliferation. Dysregulation of the multifaceted and indispensable activities of caspases has been globally linked to several diseases, including cancer and neurodegenerative disorders; however, the specific caspase members responsible for these diseases have yet to be assigned. Activity-based probes (ABPs) and peptide-based inhibitors are instrumental in the detection and control of protease activity and serve as alternative methods to genetic approaches. Such molecules aid in the interrogation of specific proteases within cellular and animal models as well as help elucidate aberrant proteolytic function correlated to disease phenotypes. No ABPs or inhibitors have been discovered that specifically target one of the eleven human caspases in a cellular context. Therefore, ascribing distinct contributions to an individual caspase activity within naturally occurring biological systems is not possible. Herein, we describe a peptide series optimized for the selective detection and inhibition of active caspase-3 in cells. These compounds exhibit low nanomolar potency against caspase-3 with >120-fold selectivity over caspase-7 which shares 77% active site identity. Our ability to individually target wild-type active caspase-3 for detection and cell permeable inhibition is a valuable proof-of-concept methodology that can be readily employed to probe the significance of caspase-3 in apoptosis, neurological disorders, cardiovascular diseases, and sepsis.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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