A Dimethylgallium Boryl Complex and Its Methyllithium Addition Compound.

The three-coordinate complex MeGa[B-(NArCH)] (Ar = CHiPr-2,6) is accessible via a tandem Lewis acid-base metathesis protocol employing (THF)Li[B(NArCH)] and GaMe. It features a very short Ga-B bond of 2.067(3) A, which was further investigated by DFT calculations and the analysis of the electron den...

Descripción completa

Detalles Bibliográficos
Publicado en:Journal of the American Chemical Society Vol. 136; no. 3; pp. 886 - 890
Autores principales: Dettenrieder, Nicole, Schädle, Christoph, Maichle-Mössmer, Cäcilia, Sirsch, Peter, Anwander, Reiner
Formato: Artículo
Publicado: American Chemical Society 1/22/2014
Materias:
Acceso en línea:Ver este registro en EBSCOhost
fields @attributes:
  recordID: 1
pdfLink:
plink: https://search.ebscohost.com/login.aspx?direct=true&db=hlh&AN=95065877&site=ehost-live
header:
  @attributes:
    shortDbName: hlh
    uiTerm: 95065877
    longDbName: Humanities International Complete
    uiTag: AN
  controlInfo:
    bkinfo:
    jinfo:
      jid:
        00027863
        ACS
      jtl: Journal of the American Chemical Society
      issn: 00027863
      maglogo: N
    pubinfo:
      dt: 1/22/2014
      vid: 136
      iid: 3
      pid: 997
      pub: American Chemical Society
    artinfo:
      ui:
        95065877
        10.1021/ja4117318
      ppf: 886
      ppct: 4
      formats:
      tig:
        atl: A Dimethylgallium Boryl Complex and Its Methyllithium Addition Compound.
      aug:
        au:
          Dettenrieder, Nicole
          Schädle, Christoph
          Maichle-Mössmer, Cäcilia
          Sirsch, Peter
          Anwander, Reiner
        affil: Institut für Anorganische Chemie, Auf der Morgenstelle 18, 72076 Tübingen, Germany
      su:
        Gallium compounds
        Methyllithium
        Electron density
        Density functionals
        Metathesis reactions
        Acid-base chemistry
        Coordination compounds
      sug:
        subj:
          Gallium compounds
          Methyllithium
          Electron density
          Density functionals
          Metathesis reactions
          Acid-base chemistry
          Coordination compounds
      ab: The three-coordinate complex MeGa[B-(NArCH)] (Ar = CHiPr-2,6) is accessible via a tandem Lewis acid-base metathesis protocol employing (THF)Li[B(NArCH)] and GaMe. It features a very short Ga-B bond of 2.067(3) A, which was further investigated by DFT calculations and the analysis of the electron density. Reaction of MeLi with MeGa[B- (NArCH)] forms tetrameric [LiMeGa{B(NArCH)}] with a "nanowheel" structure.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
    refInfo:
    copyright:
      @attributes:
        flag: Y
      dt:
        @attributes:
          year: 2014
    holdings:
      @attributes:
        islocal: N