Control of Vertex Geometry, Structure Dimensionality, Functionality, and Pore Metrics in the Reticular Synthesis of Crystalline Metal—Organic Frameworks and Polyhedra.

Metal-organic polyhedra and frameworks (MOPs and MOFs) were prepared by linking square units M(CO) (M = Cu and Zn) with a variety of organic linkers designed to control the dimensionality (periodicity) and topology of the resulting structures. We describe the preparation, characterization, and cryst...

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Publicado en:Journal of the American Chemical Society Vol. 130; no. 35; pp. 11650 - 11662
Autores principales: Furukawa, Hiroyasu, Jaheon Kim, Ockwig, Nathan W., O'keeffe, Michael, Yaghi, Omar M.
Formato: Artículo
Publicado: American Chemical Society 9/3/2008
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Acceso en línea:Ver este registro en EBSCOhost
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        10.1021/ja803783c
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        atl: Control of Vertex Geometry, Structure Dimensionality, Functionality, and Pore Metrics in the Reticular Synthesis of Crystalline Metal—Organic Frameworks and Polyhedra.
      aug:
        au:
          Furukawa, Hiroyasu
          Jaheon Kim
          Ockwig, Nathan W.
          O'keeffe, Michael
          Yaghi, Omar M.
        affil:
          Department of Chemistry and Biochemistry, Center for Reticular Chemistry at the California NanoSystems Institute, University of California, Los Angeles, California 90095-1569
          Department of Chemistry, Soongsil University, Seoul 156-743, Korea
          Geochemistry Department, Sandia National Laboratories, Albuquerque, New Mexico 87185-0754
          Department of Chemistry and Biochemistry, Arizona State University, Tempe, Arizona 85287-1604
      su:
        Structural frames
        Geometry
        Linear algebra
        Cycles
        Osmosis
      sug:
        subj:
          Structural frames
          Geometry
          Linear algebra
          Cycles
          Osmosis
      ab: Metal-organic polyhedra and frameworks (MOPs and MOFs) were prepared by linking square units M(CO) (M = Cu and Zn) with a variety of organic linkers designed to control the dimensionality (periodicity) and topology of the resulting structures. We describe the preparation, characterization, and crystal structures of 5 new MOPs and 11 new MOFs (termed MOP-14, -15, -17, -23, -24 and MOF-114, -115,-116,-117,-118,-119,-222,-601,-602,-603,-604)and show how their structures are related to the shape and functionality of the building blocks. The gas uptake behaviors of MOP-23 and MOF-601 to -603 are also presented as evidence that these structures have permanent porosity and rigid architectures.
      pubtype: Academic Journal
      doctype: Article
      src: R
    language: English
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